Tuesday, 18 June 2019

Nano Filtration


 Mass balance/Plant configuration
(NF Acid Whey)

Component
Feed
Retentate
Avg. Permeate
True Protein [%]
0.46
1.52
0.00
NPN [%]
0.16
0.28
0.07
Lactose [%]
4.77
15.36
0.11
Acid [%]
0.15
0.46
0.01
Total Ash [%]
0.78
1.32
0.35
Fat [%]
0.01
0.03
0.00
TS, Sum [%]
6.33
18.97
0.54
Phosphate PO4[%]
0.220


Calcium Ca[%]
0.086


Magnesium Mg[%]
0.009


Sulphate SO4[%]
0.012


Sodium Na [%]
0.056


Potassium K [%]
0.042


Chloride [%]
0.340


Other [%]
0.015


Cap. Avg. [l/h]
60,000
18119
65609

Key Figures
Total Protein (=True Protein + NPN) [%]                         1.80
Degree of Demineralisation[%]                                           49.07                                  
Lactose Recovery[%]                                                          98.05
Diafiltration water                                                                23728 Lit/hr                  

Feed type:

Fresh acid whey of good quality from the production of  (pH 4.5 – 4.7).

Pre-treatment:

-              Skimming to < 0.06 % fat.
-              Heat treatment at 52 - 54°C for 15 sec., or equivalent, if needed to control the bacteriological quality. (Alternatively, H2O2 (20 ppm) or sodium hydrogen sulphite (50 ppm) may be added).
-              note:
-              The temperature must not at any time exceed 60°C, as this will result in a decrease in capacity. Max. 2°C dt in the heat exchanger.
-              Adjustment to NF-plant operating temperature.
-              The inclusion of air must be avoided.
-              The addition of most types of de-foamers is not acceptable.

Operating conditions:

- Feed and retentate composition as specified.
- Feed rate: 60,000 Lit/hr
-Total feed/day: 1,080,000 Lit
- NF plant operating temperature: 10 degC
- Production time: 1x18 hr

NF Plant configuration
Membrane:     
Module:           Spiral Wound,

Loop
Spacer
No. of
Membrane elements
Area
Booster pumps
[Mil]
modules
pr. module
[m²]
Type
Installed effect
1
32
5
5
900
WHP+
30kW
2
32
5
5
900
WHP+
30kW
3
32
4
5
720
WHP+
22kW
4
32
4
5
720
WHP+
22Kw
5
32
4
5
720
WHP+
22kW
6
32
4
5
720
WHP+
22kW
Total

     

4680

148 kW
Feed and CIP pump
W+
45kW
High pressure pump 1
W+  multistage(SC)
45kW
High pressure pump 2
W+  multistage(SC)
45kW
High pressure pump3 (Diafiltration water)
CRN
45kW
Permeate pump
W+ (SC)
7.5 kW
Total effect installed

335.5 kW

SC = pumps are equipped with frequency converters

Equipment specification – NF plant

Quality stainless steel is used for all surfaces in contact with the product. All components in contact with the product are of Food and Dairy standard. The equipment specification is preliminary and changes might occur during final engineering

Twin balance tank 2x200 l incl.:
1          Loose cover
1          Level switch
2          Level transmitter

Valve manifold:

4          Change-over valves
2          Butterfly modulating valves including electro-pneumatic positioner
1          Butterfly valve with actuator

Feed pressure system:

3          Feed pumps
3          Frequency converters
1          Pressure transmitter
1          Flow transmitter including indicator
1          Triplex safety filter with automatic change over including pressure transmitters in the input and output of the filters

6          Re-circulation loops each incl.:

1          Stainless steel rack for NF modules
1          Re-circulation pump
1          Tubular heat exchanger
1          Temperature indicator
2          Pressure indicators
1          Flow indicator for permeate
1          Sampling valve

Retentate system:

1          Modulating valves
1          Flow transmitter including indicator
1          Refractometer

Permeate system:

1          Permeate pump
6          Butterfly modulating valves including electro-pneumatic positioner (APV +Kinetrol)
6          Temperature controller
Additional equipment for injecting water (Diafiltration) to the product to reach a higher level of Demineralization

Equipment for flush water:

1          Cut-off valve
1          Filter
1          Pressure switch
2          Adjustment valves

Equipment for steam and cooling water:

7          Cut-off valves
6          Regulating valves
1          Steam filter
6          Water trap
2          Non return valves
1          Temperature indicator
1          Pressure indicators
1          Multistage centrifugal pump

Soft water system:
2          Pressure indicator
2          Safety filter for water including stainless steel housing

Pipes and fittings:

Stainless steel pipes and fittings for internal connections within the NF plant
Compressed air hoses and fittings for internal connections within the NF plant

Pre-assembling

The equipment will be mounted on a stainless steel frame as a complete unit just to be connected with services and product pipes.

Fully-automatic control system:

The control panel is in mild steel and is placed in the control room. The panel is built as a PLC based control system. Two number of PC’s with 19” monitor will be utilized i.e. one for operating the plant and the other one for modifying the parameters etc. The operator will be able to monitor and supervise all of the necessary control parameters and take necessary actions from the control panel. MCC panel and electrical cables from the panel to the plant are not in the scope of supply.

The function of the panel
Automatic regulation of the level in the feed tank.
Automatic regulation of the feed pressure. The operator must adjust the pressure before the regulator is set on automatic.
Automatic regulation of the ratio of product inlet to retentate outlet (indirect regulation of TS in the retentate). The operator must adjust the ratio before the regulator is set on automatic.
Automatic regulation of the plant temperature during production and cleaning..
Automatic control of change-over valves in valve manifold.
Alarm supervision with visual alarm and action of the following:
Temperature alarm
Feed pressure alarm
Level alarm
Alarm supervision with visual alarm of the following:
Concentration alarm

The panel consists of:
PLC type Siemens (S7-414)
PLC based control system
Various power supplies, fuses and clamps

Operating principles
The plant is mainly operated from the panel and partly by operating service valves etc. directly on the plant. On the monitor you can see the process values, which is a part of the regulation loop. During start and stop of the plant and during start and stop of production the operator must carry out some operation on the OP panel, but during production and CIP the plant is self-supervised and is able to take action on account of possible alarms.




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